AMaCC platform – Equipments

The platform has an area of 125m², including 90m² of laboratories in which all the analytical equipment is distributed. It was financed with the support of:

europe region pdll

The operation CPER "Spectrométrie de masse CEISAM" of the project CISPEO is cofunded by the European Union through the funds of the region Pays de la Loire (FEDER).

UPLC-MS² high resolution (Waters)

UPLC: Acquity H-Class
MS: ESI-Q-TOF (XEVO G2-XS QTOF)
Analysis: MS, mesure de masse exacte (HRMS), MS², UPLC-MS, UPLC-MS²
Sources/probes: ESI/APCI, ASAP
Introduction modes: liquid or solid

GC-MS basse résolution (Agilent)

GC-MS low resolution (Agilent)

GC: 7890B
MS: IE-SQ (MSD5977B)
Analysis:  GC-MS, characterization of small organic molecules using library screening
Source: EI
Introduction mode : liquid

Reverse-Phase HPLC (Waters)

HPLC: Alliance e2695
Detection 1: UV-VIS diode array (PDA 2996)
Detection 2: DEDL (ELS 2424)
Detection 3: Multifluorescence Detector (FLD 2475)
Analyses: Molecular characterization, assays, monitoring of organic synthesis

HPLC Chirale (Agilent)

HPLC Chirale (Agilent)

HPLC: 1100 Agilent
Detector 1:  UV-VIS with diode array (Agilent)
Detector 2: Polarimètre OR 2090 (JASCO)
Injection mode : autosampler
Separation mode: chirale, normale phase
Analyses: quantitative analysis of enantiomeric excess, diastereomeric ratios measurement

Screening with 9 chiral columns:

CHIRALPAK AD-H, AS-H, IA, IB, IC
CHIRALCEL OD-H, OJ-H
Lux Amylose-2
Lux Cellulose-4

UPLC dual detection (Waters)

UPLC : Acquity H-Class
Detector 1: DEDL
Detector 2: UV-VIS with diode array
Separation mode: reversed phase, HILIC
Analysis: characterization of molecules, quantitative analysis, monitoring of kinetic reactions

Ion Chromatography (Metrohm)

HPLC: Metrohm 883 Basic IC
Detection: Conductivity
Suppressor: MSM A module
Injection mode: Manual
Analyses: Measurement and quantification of anions and cations down to the µg/L range

Self-Service Tools

Self-Service HPLC (Agilent)

HPLC: Agilent 1200 Series
Detection: UV-Vis
Injection mode: Manual
Separation mode: Reverse-phase
Analyses: Molecular characterization, monitoring of organic synthesis

3 GC-FID Automatic injection (Agilent)

GC: 7820 and 6890
Detector: FID
Injection mode: Split/Splitless autosampler
Analysis: characterization of molecules, organic synthesis monitoring, monitoring of kinetic reactions, quantitative analysis

GC-TCD (Agilent)

GC: 6890
Detector: TCD
Injection mode: Split/Splitless (manual)
Analysis: quantitative measurement of H2, CO, and CO2

GC manual injection (Agilent)

GC : 6890
Detector: FID
Injection mode: Split/Splitless (manual)
Analysis: measurement of acetylene and ethylene